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Syllabus:

Advanced Experimental Tools in Chemistry, 15 Credits

The course is discontinued from 2021-08-09

Swedish name: Avancerade experimentella kemiska verktyg

This syllabus is valid: 2014-07-07 and until further notice

Course code: 5KE144

Credit points: 15

Education level: Second cycle

Main Field of Study and progress level: Chemistry: Second cycle, in-depth level of the course cannot be classified

Grading scale: Three-grade scale

Responsible department: Department of Chemistry

Revised by: Faculty Board of Science and Technology, 2021-08-09

Contents

Advanced experimental and instrumental chemical techniques play a decisive role for studies of molecules and their interaction with their surroundings. Chemists are supposed to possess the ability to both produce completely new substances and to study these with the help of suitable tools - a combination of knowledge that is central within many natural scientific, medical and technological disciplines within both academia and industry. The course addresses theoretical and practical aspects of modern techniques for producing, isolating and characterising various types of chemical substances that are important within the life and environmental sciences. The course encompasses four modules that address tools for (i) synthesis and isolation, (ii) separation, (iii) identification and quantification, (iv) structure-characterisation. The course focuses on liquid chromatography,mass spectrometry, infrared and Raman spectroscopy, and techniques for x-ray spectroscopy and x-ray diffraction. The course's laboratory experiments cover organic synthesis work and practical work with advanced chemical instrumentation. They are closely connected with ongoing research at Umeå University within the fields of protein, medicinal and environmental chemistry.

Expected learning outcomes

fter completing the course, students shall be able to:

describe and compare choices of applicable techniques within organic synthesis
explain the theoretical and practical conditions that enable or limit usage of the chromatographic and spectroscopic techniques addressed by the course.
decide how the chemical and physical qualities of a chemical compound, and how the technical design of the measuring instrument, affect performance parameters such as signal intensity, signal profile, detectability and selectivity, as well as the occurrence and correction of interferences.
assess which type of information can be extracted from experiments using the spectroscopic techniques addressed on the course, and how such information can provide knowledge regarding chemical structure, speciation and a substance's redox state.
critically evaluate and practically use concepts for validation, quality control and determining of the measurement uncertainty of analysis results.
independently analyse data from a selection of spectroscopic experiments addressed on the course. argue for choice of suitable separation and analysis techniques for a specific chemical problem.
plan and conduct laboratory work in accordance with a scientific way of working, including risk assessment, and document laboratory work in a correct and reliable manner.
present and discuss the results received in English in the form of a poster, for various groups
critically discuss fundamental issues associated with scientific theory and standpoints, from a societal perspective.

Required Knowledge

Passed courses in Chemistry, 60 credits, and the course Biophysical-Chemical Concepts(15 credits, 5KE145), or the equivalent. Proficiency in English equivalent to Swedish upper secondary course English A (IELTS (Academic) with a minimum overall score of 5.5 and no individual score below 5.0. TOEFL PBT (Paper-based Test) with a minimum total score of 530 and a minimum TWE score of 4. TOEFL iBT (Internet-based Test) with a minimum total score of 72 and a minimum score of 17 on the Writing Section). Where the language of instruction is Swedish, applicants must prove proficiency in Swedish to the level required for basic eligibility for higher studies.

Form of instruction

The teaching may take the form of lectures, lessons, tutorials, self-tuition and laboratory experiments. The laboratory experiments and associated group exercises are mandatory.

Examination modes

Examinations are conducted partly through a written examination and partly through written and verbal reports of laboratory experiments, the latter in addition through a poster presentation. For the laboratory experiments, the following grades are awarded: Fail (U), or Pass (G). For written examinations, the grades Fail (U), Pass (G) or Pass with distinction (VG) are awarded. For the whole course, the grades Fail (U), Pass (G) or Pass with distinction (VG) are awarded. To pass the whole course, all examinations and obligatory elements must have been passed. Those who pass an examination may not take the same examination again with the aim of achieving a higher grade. A student who has taken two examinations for a course or a part of a course, without passing either examination, has the right to have another examiner appointed, if there are no specific reasons for not doing so (Chapter 6, Section 22, HEA). Requests for a different examiner are to be made to the Head of the Department of Chemistry.

Other regulations

Students are entitled to an assessment of whether previous education or equivalent knowledge and skills acquired in professional experience can be accredited for equivalent studies at Umeå University. Applications for credit transfers must be sent to Student Services/Degree Evaluation Office. More information on credit transfers can be found on Umeå University's student web, www.student.umu.se, and in the Higher Education Ordinance (Chapter 6). Rejected applications for credit transfers can be appealed (Higher Education Ordinance, Chapter 12) to the Higher Education Appeals Board. This applies whether the rejection relates to all or parts of the credit transfer application.

Literature

The literature list is not available through the web. Please contact the faculty.